Crystal structure of the twinned tetramethylurea adduct of 2-phenyl-1,3-dioxa-2-borolane-4,5-dione
| العنوان: | Crystal structure of the twinned tetramethylurea adduct of 2-phenyl-1,3-dioxa-2-borolane-4,5-dione |
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| المؤلفون: | Peter Paetzold, Stephan Neyses, Ulli Englert |
| المصدر: | Structural Chemistry. 5:51-55 |
| بيانات النشر: | Springer Science and Business Media LLC, 1994. |
| سنة النشر: | 1994 |
| مصطلحات موضوعية: | Crystallography, Chemistry, Tetramethylurea, X-ray crystallography, Crystal structure, Lewis acids and bases, Physical and Theoretical Chemistry, Condensed Matter Physics, Crystal twinning, Monoclinic crystal system, Adduct |
| الوصف: | The title compound crystallizes in the monoclinic space groupP21/c. Twinning occurs between domains sharing thehk0 zone. The indices of imprecise intensity data were interpreted successfully. A subset of these data could be corrected and used in structure determination together with single-crystal intensity data of the predominant domain, whereas the remaining superposition data were excluded from refinement. Structure solution converged at satisfactory values ofR=0.082,Rw=0.074. The structure consists of isolated Lewis acid base adducts. |
| تدمد: | 1572-9001 1040-0400 |
| الوصول الحر: | https://explore.openaire.eu/search/publication?articleId=doi_________::2c538772fd71f3e72fb6c8a9dc40b13fTest https://doi.org/10.1007/bf02278695Test |
| حقوق: | CLOSED |
| رقم الانضمام: | edsair.doi...........2c538772fd71f3e72fb6c8a9dc40b13f |
| قاعدة البيانات: | OpenAIRE |
| تدمد: | 15729001 10400400 |
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