دورية أكاديمية

Detailed example of the identification and crystallographic analysis of a pseudo-merohedrally twinned crystal.

التفاصيل البيبلوغرافية
العنوان: Detailed example of the identification and crystallographic analysis of a pseudo-merohedrally twinned crystal.
المؤلفون: Guzei, Ilia, Herbst-Irmer, Regine, Munyaneza, Apollinaire, Darkwa, James
المصدر: Acta Crystallographica: Section B (Wiley-Blackwell). Apr2012, Vol. 68 Issue 2, p150-157. 8p.
مصطلحات موضوعية: *CRYSTALLOGRAPHY, *X-ray crystallography technique, *CRYSTAL structure, *ORGANOMETALLIC compounds spectra, *TWINNING (Crystallography)
مستخلص: A detailed description of the procedures utilized in the non-routine X-ray single-crystal structural determination and refinement of a pseudo-merohedrally twinned crystal of an Fe/Ni organometallic complex is presented. It illustrates to the practitioners of crystallography how to properly handle such cases and describes the logic and concrete steps necessary to account for the twinning, pseudo-symmetry and atomic positional disorder. [ABSTRACT FROM AUTHOR]
قاعدة البيانات: Academic Search Index
الوصف
تدمد:01087681
DOI:10.1107/S0108768112002728