دورية أكاديمية
Synthesis and evaluation of polymeric continuous bed (monolithic) reversed-phase gradient stationary phases for capillary liquid chromatography and capillary electrochromatography ; Ištisinių (monolitinių) atvirkščių fazių gradientinių sorbentų, skirtų kapiliarinei skysčių chromatografijai ir kapiliarinei elektrochromatografijai, sintezė ir įvertinimas
| العنوان: | Synthesis and evaluation of polymeric continuous bed (monolithic) reversed-phase gradient stationary phases for capillary liquid chromatography and capillary electrochromatography ; Ištisinių (monolitinių) atvirkščių fazių gradientinių sorbentų, skirtų kapiliarinei skysčių chromatografijai ir kapiliarinei elektrochromatografijai, sintezė ir įvertinimas |
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| المؤلفون: | Maruška, Audrius, Rocco, Anna, Kornyšova, Olga, Fanali, Salvatore |
| سنة النشر: | 2007 |
| المجموعة: | Vytautas Magnus University e-Publication Repository (VMU ePub) / Vytauto Didžiojo universitetas: e. publikacijų talpykla (VDU ePub) |
| مصطلحات موضوعية: | Gradient stationary phase, Continuous bed, Monolith, Capillary liquid chromatography, Capillary electrochromatography, Microchip, Reversed-phase, Straipsnis Clarivate Analytics Web of Science / Article in Clarivate Analytics Web of Science (S1), Chemija / Chemistry (N003) |
| جغرافية الموضوع: | NL |
| الوصف: | There is a demand of novel high resolution separation media for separation of complex mixtures, particularly biological samples. One of the most flexible techniques for development of new separation media currently is synthesis of the continuous bed (monolithic) stationary phases. In this study the capillary format gradient stationary phases were formed using continuous bed (monolith) polymerization in situ. Different reversed-phase stationary phase gradients were tailored and their resolution using capillary liquid chromatography and capillary electrochromatography at isocratic mobile phase conditions was evaluated. It is demonstrated, that efficiency and resolution of the gradient stationary phases can be substantially increased comparing to the common (isotropic) stationary phases. The proposed formation approach of the gradient stationary phase is reproducible and compatible with the capillary format or microchip format separations. It can be easily automated for the separation optimizations or mass production of the capillary columns or chips ; Vytauto Didžiojo universitetas |
| نوع الوثيقة: | article in journal/newspaper |
| وصف الملف: | p. 47-55; text/xml |
| اللغة: | English |
| ردمك: | 978-0-00-245001-0 0-00-245001-1 |
| تدمد: | 0165022X |
| العلاقة: | Journal of biochemical and biophysical methods. Amsterdam : Elsevier B.V., 2007, Vol. 70, iss. 1; Science Citation Index Expanded (Web of Science); INSPEC; MEDLINE; Chemical Abstracts (CAplus); ScienceDirect; Scopus; VDU02-000002879; https://doi.org/10.1016/j.jbbm.2006.10.011Test; WOS:000245001100007 |
| DOI: | 10.1016/j.jbbm.2006.10.011 |
| الإتاحة: | https://doi.org/10.1016/j.jbbm.2006.10.011Test |
| رقم الانضمام: | edsbas.AFFFF1D3 |
| قاعدة البيانات: | BASE |
| ردمك: | 9780002450010 0002450011 |
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| تدمد: | 0165022X |
| DOI: | 10.1016/j.jbbm.2006.10.011 |