دورية أكاديمية

Laboratory comparison of field portable X-ray fluorescence spectrometer (FP-XRF) and inductively coupled plasma mass spectrometry (ICP-MS) for determination of airborne metals in stainless steel welding fume.

التفاصيل البيبلوغرافية
العنوان: Laboratory comparison of field portable X-ray fluorescence spectrometer (FP-XRF) and inductively coupled plasma mass spectrometry (ICP-MS) for determination of airborne metals in stainless steel welding fume.
المؤلفون: Newton, Ashley1, Rule, Ana M.1, Serdar, Berrin2, Koehler, Kirsten1 kkoehle1@jhu.edu
المصدر: Journal of Occupational & Environmental Hygiene. Nov2023, Vol. 20 Issue 11, p536-544. 9p.
مصطلحات موضوعية: *METAL analysis, *AIR pollution, *CLINICAL pathology, *PARTICULATE matter, *OCCUPATIONAL exposure, *COMPARATIVE studies, *MANGANESE, *X-ray spectroscopy, *MASS spectrometry, *DESCRIPTIVE statistics, *RESEARCH funding, *COPPER, *ZINC, *METALLURGY
مصطلحات جغرافية: IDAHO
مستخلص: Welding fume is a common exposure in occupational settings. Gravimetric analysis for total particulate matter is common; however, the cost of laboratory analyses limits the availability of quantitative exposure assessment for welding fume metal constituents in occupational settings. We investigated whether a field portable X-ray fluorescence spectrometer (FP-XRF) could provide accurate estimates of personal exposures to metals common in welding fume (chromium, copper, manganese, nickel, vanadium, and zinc). The FP-XRF requires less training and is easier to deploy in many settings than traditional wet laboratory analyses. Filters were analyzed both by FP-XRF and inductively coupled plasma mass spectrometry (ICP-MS). We estimated the FP-XRF limit of detection for each metal and developed a correction factor accounting for the non-uniform deposition pattern on filter samples collected with an Institute of Medicine (IOM) inhalable particulate matter sampler. Strong linear correlation was observed for all metals (0.72
قاعدة البيانات: Academic Search Index
الوصف
تدمد:15459624
DOI:10.1080/15459624.2023.2244022