Determination of propylthiouracil at a nanomolar level using Fast Fourier transformation continuous cyclic voltammetry under flow conditions

التفاصيل البيبلوغرافية
العنوان: Determination of propylthiouracil at a nanomolar level using Fast Fourier transformation continuous cyclic voltammetry under flow conditions
المؤلفون: Norouzi, P., Ganjali, M. R., Sehat, A. A., Mirahmadi, S., Larijani, B.
المصدر: Chemia Analityczna.
مصطلحات موضوعية: propylotiouracyl, transformacja Fouriera szybka, analiza wstrzykowo-przepływowa, ultramikroelektroda, woltamperometria cykliczna, propylthiouracyl, fast Fourier transformation, ultramicroelectrodes, cyclic voltammetry
الوصف: Asimple, fast, and economical Fast Foiirier Transformation Continuous Cyclic Voitammetric technique (FFTCV) for determinatipn of propylthiouracyl in pharmaceutical formulation under flow-injection conditions has been developed. The proposed method is also precise, accurate, sensitive, and selective. Potential waveform comprising consecutive potential steps for cleaning, accumulation, and redox reaction of the anaiyte was applied to Au disk micro-electrode. The effect of eluent's pH, accumulation potential, sweep rate, and accumulation time were considered. The method was linear in the analyte's concentration range of 20-3230 pg mL-1(r = 0.998; detection and determination limits were 6 and 20 pg mL-1respectively). The proposed method is advantageous to other methods with two respects: fast determination rate, and no requirement for oxygen removal from the solution.
نوع الوثيقة: Article
اللغة: English
الوصول الحر: http://yadda.icm.edu.pl/baztech/element/bwmeta1.element.baztech-article-BPP1-0075-0004Test
رقم الانضمام: edsbzt.bwmeta1.element.baztech.article.BPP1.0075.0004
قاعدة البيانات: BazTech