Fabrication of Cu1.5Mn1.5O4 Nanoparticles Using One Step Self-Assembling Route to Enhance Energy Consumption
| العنوان: | Fabrication of Cu1.5Mn1.5O4 Nanoparticles Using One Step Self-Assembling Route to Enhance Energy Consumption |
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| المؤلفون: | Omar H. Abd-Elkader, Ghadah M. Al-Senani, Nasrallah M. Deraz |
| المصدر: | Applied Sciences, Vol 11, Iss 2034, p 2034 (2021) Applied Sciences Volume 11 Issue 5 |
| بيانات النشر: | MDPI AG, 2021. |
| سنة النشر: | 2021 |
| مصطلحات موضوعية: | Materials science, Fourier-transform infrared (FTIR), Scanning electron microscope, Nanoparticle, 02 engineering and technology, engineering.material, 010402 general chemistry, 01 natural sciences, X-ray diffraction (XRD), lcsh:Technology, Cu1.5Mn1.5O4 nanoparticles (NPs), transmittance electron micrograph (TEM), lcsh:Chemistry, Hopcalite, chemistry.chemical_compound, energy-dispersive spectroscopy (EDS), scanning electron microscope (SEM), vibrating sample magnetometer (VSM), General Materials Science, Ceramic, Instrumentation, lcsh:QH301-705.5, Fluid Flow and Transfer Processes, lcsh:T, Process Chemistry and Technology, Spinel, General Engineering, 021001 nanoscience & nanotechnology, Manganite, Nanocrystalline material, lcsh:QC1-999, 0104 chemical sciences, Computer Science Applications, chemistry, Chemical engineering, lcsh:Biology (General), lcsh:QD1-999, lcsh:TA1-2040, visual_art, engineering, visual_art.visual_art_medium, Crystallite, 0210 nano-technology, lcsh:Engineering (General). Civil engineering (General), lcsh:Physics |
| الوصف: | The preparation of copper manganite (hopcalite, Cu1.5Mn1.5O4), as a single phase, was achieved by using a sustainable method of green synthesis. This method is based on the replacement of the conventional “brute force” ceramic preparation by the recent “soft force” green synthesis via the egg white assisted one-step method. In other words, we present a facile and rapid methodology to prepare the nanocrystalline Cu1.5Mn1.5O4 spinel as a single phase, compared to our previous work using ceramic and glycine-assisted combustion methods. The as-synthesized copper manganite was characterized using X-ray diffraction (XRD), Fourier-transform infrared (FTIR), energy-dispersive spectroscopy (EDS), and scanning electron microscope (SEM). We used a vibrating sample magnetometer to determine the magnetic properties of the prepared sample (VSM). XRD, FTIR, SEM, EDS and transmittance electron micrograph (TEM) resulted in synthesis of a successful cubic spinel Cu1.5Mn1.5O4 system with a sponge crystal structure. The particles of the prepared materials are polycrystalline in their nature and the sizes ranged between 50 and 100nm. The magnetic measurement demonstrated that the generated nanostructure has been found to exhibit ferromagnetism at room temperature with an optimum saturation magnetization value (0.2944 emu/g). |
| وصف الملف: | application/pdf |
| اللغة: | English |
| تدمد: | 2076-3417 |
| الوصول الحر: | https://explore.openaire.eu/search/publication?articleId=doi_dedup___::b5829fb36772c2604d080dc87ca17c31Test https://www.mdpi.com/2076-3417/11/5/2034Test |
| حقوق: | OPEN |
| رقم الانضمام: | edsair.doi.dedup.....b5829fb36772c2604d080dc87ca17c31 |
| قاعدة البيانات: | OpenAIRE |
| تدمد: | 20763417 |
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