التفاصيل البيبلوغرافية
| العنوان: |
Metal-Organic Frameworks to Metal/Metal Oxide Embedded Carbon Matrix: Synthesis, Characterization and Gas Sorption Properties. |
| المؤلفون: |
Jiun-Jen Chen, Ya-Ting Chen, Raja, Duraisamy Senthil, Yu-Hao Kang, Pen-Chang Tseng, Chia-Her Lin |
| المصدر: |
Materials (1996-1944); 2015, Vol. 8 Issue 8, p5336-5347, 18p, 3 Color Photographs, 3 Black and White Photographs, 1 Chart, 16 Graphs |
| مصطلحات موضوعية: |
METAL organic chemical vapor deposition, METALLIC oxides, X-ray spectroscopy, X-ray diffraction, CARBONIZATION |
| مستخلص: |
Three isostructural metal-organic frameworks, (MOFs), [Fe(OH)(1,4-NDC)] (1), [Al(OH)(1,4-NDC)] (2), and [In(OH)(1,4-NDC)] (3) have been synthesized hydrothermally by using 1,4-naphthalene dicarboxylate (1,4-NDC) as a linker. The MOFs were characterized using various techniques and further used as precursor materials for the synthesis of metal/metal oxide nanoparticles inserted in a carbon matrix through a simple thermal conversion method. The newly synthesized carbon materials were characterized by scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectroscopy analysis, powder X-ray diffraction and BET analysis. The results showed that the MOF-derived carbon composite materials maintained the morphology of the original MOF upon carbonization, and confirmed the insertion of metal/metal oxide particles in the carbon matrix. [ABSTRACT FROM AUTHOR] |
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