دورية أكاديمية
Determination of Budesonide and Sulfasalazine in Water and Wastewater Samples Using DLLME-SFO-HPLC-UV Method
| العنوان: | Determination of Budesonide and Sulfasalazine in Water and Wastewater Samples Using DLLME-SFO-HPLC-UV Method |
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| المؤلفون: | Hryniewicka, Marta, Starczewska, Barbara, Gołębiewska, Agnieszka |
| بيانات النشر: | MDPI |
| سنة النشر: | 2019 |
| المجموعة: | Repozytorium Uniwersytetu w Białymstoku (RUB) |
| مصطلحات موضوعية: | budesonide, sulfasalazine, 1-undecanol, DLLME-SFO, HPLC-UV |
| الوصف: | Dispersive liquid–liquid microextraction based on solidification of floating organic droplet (DLLME-SFO) was applied to isolate budesonide (BUD) and sulfasalazine (SULF) from aqueous samples. The effects of different parameters on the efficiency on the extraction such as type of extrahent and dispersive solvent, ionic strength, pH of sample, and centrifugation time were investigated. Moreover, the influence of foreign substances on a studied process was tested. The calibration curves were recorded. The linearity ranges for BUD and SULF were 0.022–8.611 µg mL−1 and 0.020–7.968 µg mL−1 with the limit of detection (LOD) 0.011 µg mL−1 and 0.012 µg mL−1 , respectively. The enrichment factors (EF) for two analytes were high: for BUD it was 145.7 and for SULF, 119.5. The elaborated procedure was applied for HPLC-UV determination of these analytes in water and wastewater samples. ; Marta Hryniewicka: martah@uwb.edu.pl ; Marta Hryniewicka - Institute of Chemistry, University of Białystok, ul. Ciołkowskiego 1K, 15-245 Białystok, Poland ; Semreen, M.H.; Shanableh, A.; Semerjian, L.; Alniss, H.; Mousa, M.; Bai, X.; Acharya, K. Simultaneous Determination of Pharmaceuticals by Solid-phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry: A Case Study from Sharjah Sewage Treatment Plant. Molecules 2019, 24, 633. ; Wang, Y.; Tang, Y.; Moellmann, H.; Hochhaus, G. Simultaneous quantification of budesonide and its two metabolites, 6beta-hydroxybudesonide and 16alpha-hydroxyprednisolone, in human plasma by liquid chromatography negative electrospray ionization tandem mass spectrometry. Biomed. Chromatogr. 2003, 17, 158–164. ; Gazzotti, T.; Barbarossa, A.; Zironi, E.; Roncada, P.; Pietra, M.; Pagliuca, G. An LC-MS/MS method for the determination of budesonide and 16 alpha-hydroxyprednisolone in dog plasma. Methodsx 2016, 3, 139–143. ; Graham, G.G.; Pile, K.D. Sulfasalazine and Related Drugs; Encyclopedia of Inflammatory Diseases; Springer: New York, NY, USA, 2014; pp. 1–5. ; Gupta, M.; Bhargava, H.N. Development and ... |
| نوع الوثيقة: | article in journal/newspaper |
| وصف الملف: | application/pdf |
| اللغة: | English |
| تدمد: | 2073-4441 |
| العلاقة: | Water, vol. 11, no. 8, 2019, p. 1-14; http://hdl.handle.net/11320/16424Test; Water |
| DOI: | 10.3390/w11081581 |
| الإتاحة: | https://doi.org/10.3390/w11081581Test http://hdl.handle.net/11320/16424Test |
| حقوق: | Attribution 4.0 International ; https://creativecommons.org/licenses/by/4.0Test/ ; © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0Test/). |
| رقم الانضمام: | edsbas.B5556239 |
| قاعدة البيانات: | BASE |
Full Text Finder | تدمد: | 20734441 |
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| DOI: | 10.3390/w11081581 |